2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

Base Information

Chemical Name:2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran
CAS No.:796072-21-4
Molecular Formula:C₃₄H₃₃NO₄
Molecular Weight:519.64
Hs Code.:

Synonyms:2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

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Chemical Property of 2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

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Technology Process of 2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

There total 6 articles about 2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 796072-20-3
2-butyl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-benzofuran

: 796072-42-9
4-bromo-2-nitro-1-(3-phenylpropyloxy)-benzene

: 796072-21-4
2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

Guidance literature:: With potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In DMF (N,N-dimethyl-formamide); water; at 120 ℃;

Reference yield:

: 4265-27-4
2-n-butylbenzo[b]furan

: 796072-21-4
2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

Guidance literature:: Multi-step reaction with 5 steps

1: aluminum (III) chloride / 3 h / 0 °C

2: sodium tetrahydroborate / ethanol / 1 h / 0 °C

3: triethylsilane; trifluoroacetic acid / dichloromethane / 3 h / 0 °C

4: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 80 °C

5: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; N,N-dimethyl-formamide / 120 °C

With triethylsilane; aluminum (III) chloride; sodium tetrahydroborate; potassium acetate; potassium carbonate; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 4: Suzuki Coupling / 5: Suzuki Coupling;

Reference yield:

: 796072-19-0
3-(4-bromo-benzyl)-2-butyl-benzofuran

: 796072-21-4
2-butyl-3-[3'-nitro-4'-(3-phenyl-propoxy)-biphenyl-4-ylmethyl]-benzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 80 °C

2: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; N,N-dimethyl-formamide / 120 °C

With potassium acetate; potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: Suzuki Coupling / 2: Suzuki Coupling;