Technology Process of 4-amino-3-benzylcoumarin
There total 12 articles about 4-amino-3-benzylcoumarin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 76 percent / conc. sulphuric acid / 20 h / Heating
2: 70 percent / sodium metaperiodate / H2O; methanol / 18 h / 50 °C
3: 84 percent / NaOH / 5 h / other reagent
4: 73 percent / 60percent sodium hydride / toluene / Ambient temperature
5: 90 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature
6: 75 percent / H2 / 5percent Pd-C / methanol
With
sodium hydroxide; sodium periodate; hydrogen; sodium hydride;
palladium on activated charcoal; sulfuric acid;
In
methanol; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 70 percent / sodium metaperiodate / H2O; methanol / 18 h / 50 °C
2: 84 percent / NaOH / 5 h / other reagent
3: 73 percent / 60percent sodium hydride / toluene / Ambient temperature
4: 90 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature
5: 75 percent / H2 / 5percent Pd-C / methanol
With
sodium hydroxide; sodium periodate; hydrogen; sodium hydride;
palladium on activated charcoal;
In
methanol; water; N,N-dimethyl-formamide; toluene;