C₅₃H₆₀O₁₉N₄S₂

Base Information

Chemical Name:C₅₃H₆₀O₁₉N₄S₂
CAS No.:945224-51-1
Molecular Formula:C₅₃H₆₀N₄O₁₉S₂
Molecular Weight:1121.21
Hs Code.:

C<sub>53</sub>H<sub>60</sub>O<sub>19</sub>N<sub>4</sub>S<sub>2</sub>

Synonyms:C₅₃H₆₀O₁₉N₄S₂

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Chemical Property of C₅₃H₆₀O₁₉N₄S₂

Chemical Property:

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Technology Process of C₅₃H₆₀O₁₉N₄S₂

There total 21 articles about C₅₃H₆₀O₁₉N₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 945224-50-0
N-(benzyl)-N-benzyloxycarbonyl-5-aminopentyl (2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

: 945224-51-1
C₅₃H₆₀O₁₉N₄S₂

Guidance literature:: With triethylamine sulfurtrioxide; In pyridine; at 20 ℃; for 4h;
DOI:10.1002/chem.200700141

Reference yield:

: 945224-35-1
2-O-pivaloyl-3-O-benzyl-4-O-levulinoyl-5-O-triphenylmethyl-D-xylose di(ethylthio)acetal

: 945224-51-1
C₅₃H₆₀O₁₉N₄S₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: 90 percent / triethylsilane; trifluoroacetic acid / CH₂Cl₂ / 0.08 h

2.1: 94 percent / sulfur trioxide pyridine complex; DIPEA; dimethyl sulfoxide / CH₂Cl₂ / 0.25 h / 0 °C

3.1: MgBr₂*OEt₂ / CH₂Cl₂ / 20 °C

3.2: 73 percent / hydrazine acetate / CH₂Cl₂; methanol / 12 h / 20 °C

4.1: acetyl chloride / toluene / 0 - 20 °C

4.2: 70 percent / water / toluene / 0 - 20 °C

5.1: 4-dimethylaminopyridine; N,N'-diisopropylcarbodiimide / CH₂Cl₂ / 2.5 h / 0 °C

6.1: bis(trifluoroacetoxy)iodobenzene; water; NaHCO₃ / acetonitrile / 0.5 h / 20 °C

6.2: trifluoroacetic acid / H₂O / 0.5 h / 50 °C

7.1: 461 mg / DBU / CH₂Cl₂ / 0.5 h / 0 - 20 °C

8.1: TMSOTf / CH₂Cl₂ / 0.5 h / -20 - -10 °C

9.1: 96 percent / pyridine; acetic acid; hydrazine monohydrate / CH₂Cl₂ / 1.5 h / 20 °C

10.1: 81 percent / TMSOTf / CH₂Cl₂ / 0.5 h / -25 °C

11.1: H₂O₂; LiOH; H₂O / tetrahydrofuran / 16 h / 20 °C

11.2: 85 percent / aq. KOH; MeOH / tetrahydrofuran / 16 h / 20 °C

12.1: 82 percent / SO₃*Et₃N / pyridine / 4 h / 20 °C

With pyridine; triethylsilane; dmap; lithium hydroxide; trimethylsilyl trifluoromethanesulfonate; water; dihydrogen peroxide; triethylamine sulfurtrioxide; sulfur trioxide pyridine complex; sodium hydrogencarbonate; hydrazine hydrate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; acetyl chloride; trifluoroacetic acid; bis-[(trifluoroacetoxy)iodo]benzene; magnesium bromide; diisopropyl-carbodiimide; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; pyridine; dichloromethane; toluene; acetonitrile; 2.1: Parikh-Doering oxidation / 4.1: Pinner reaction;
DOI:10.1002/chem.200700141

Reference yield:

: 945224-43-1
C₂₆H₃₈O₇S₂

: 945224-51-1
C₅₃H₆₀O₁₉N₄S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: MgBr₂*OEt₂ / CH₂Cl₂ / 20 °C

1.2: 73 percent / hydrazine acetate / CH₂Cl₂; methanol / 12 h / 20 °C

2.1: acetyl chloride / toluene / 0 - 20 °C

2.2: 70 percent / water / toluene / 0 - 20 °C

3.1: 4-dimethylaminopyridine; N,N'-diisopropylcarbodiimide / CH₂Cl₂ / 2.5 h / 0 °C

4.1: bis(trifluoroacetoxy)iodobenzene; water; NaHCO₃ / acetonitrile / 0.5 h / 20 °C

4.2: trifluoroacetic acid / H₂O / 0.5 h / 50 °C

5.1: 461 mg / DBU / CH₂Cl₂ / 0.5 h / 0 - 20 °C

6.1: TMSOTf / CH₂Cl₂ / 0.5 h / -20 - -10 °C

7.1: 96 percent / pyridine; acetic acid; hydrazine monohydrate / CH₂Cl₂ / 1.5 h / 20 °C

8.1: 81 percent / TMSOTf / CH₂Cl₂ / 0.5 h / -25 °C

9.1: H₂O₂; LiOH; H₂O / tetrahydrofuran / 16 h / 20 °C

9.2: 85 percent / aq. KOH; MeOH / tetrahydrofuran / 16 h / 20 °C

10.1: 82 percent / SO₃*Et₃N / pyridine / 4 h / 20 °C

With pyridine; dmap; lithium hydroxide; trimethylsilyl trifluoromethanesulfonate; water; dihydrogen peroxide; triethylamine sulfurtrioxide; sodium hydrogencarbonate; hydrazine hydrate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride; bis-[(trifluoroacetoxy)iodo]benzene; magnesium bromide; diisopropyl-carbodiimide; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; pyridine; dichloromethane; toluene; acetonitrile; 2.1: Pinner reaction;
DOI:10.1002/chem.200700141