1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil

Base Information

Chemical Name:1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil
CAS No.:88425-51-8
Molecular Formula:C₂₀H₁₇Br₂N₅O₇
Molecular Weight:599.192
Hs Code.:

Synonyms:1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil

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Technology Process of 1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil

There total 2 articles about 1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67014-24-8
3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-D-arabinofuranosyl chloride

: 5-(2,2-Dibromo-vinyl)-1-trimethylsilanyl-1H-pyrimidine-2,4-dione

: 88425-55-2
1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-α-D-arabinofuranosyl)-5-dibromovinyluracil

: 88425-51-8
1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil

Guidance literature:: With mercury dibromide; In 1,2-dichloro-ethane; at 50 - 55 ℃; for 72h; Yield given. Yields of byproduct given;
DOI:10.1021/jm00369a032

Reference yield:

: 61135-31-7
5-(2,2-dibromovinyl)-uracil

: 88425-51-8
1-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-azido-β-D-arabinofuranosyl)-5-dibromovinyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: Heating

2: HgBr₂ / 1,2-dichloro-ethane / 72 h / 50 - 55 °C

With mercury dibromide; In 1,2-dichloro-ethane;
DOI:10.1021/jm00369a032