methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

Base Information

Chemical Name:methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside
CAS No.:147314-71-4
Molecular Formula:C₁₄H₁₉N₃O₆S
Molecular Weight:357.387
Hs Code.:

Synonyms:methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

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Technology Process of methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

There total 3 articles about methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 147314-68-9
methyl 3-azido-3-deoxy-5-O-methyl-β-D-xylofuranoside

: 98-59-9
p-toluenesulfonyl chloride

: 147314-71-4
methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

Guidance literature:: With pyridine; for 48h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80332-X

Reference yield:

: 60761-87-7
methyl 5-O-methyl-β-D-ribofuranoside

: 147314-71-4
methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / thionyl chloride, triethylamine / tetrahydrofuran / 3 h / 0 °C

2: 55 percent / sodium azide / dimethylformamide / 48 h / Heating

3: 93 percent / pyridine / 48 h / Ambient temperature

With pyridine; thionyl chloride; sodium azide; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80332-X

Reference yield:

: methyl 5-O-methyl-2,3-O-sulfinyl-β-D-ribofuranoside

: 147314-71-4
methyl 3-azido-3-deoxy-5-O-methyl-2-O-p-toluenesulfonyl-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / sodium azide / dimethylformamide / 48 h / Heating

2: 93 percent / pyridine / 48 h / Ambient temperature

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80332-X