2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

Base Information

Chemical Name:2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate
CAS No.:1192165-17-5
Molecular Formula:C₂H₄O₂*C₁₇H₂₅N₃O
Molecular Weight:347.458
Hs Code.:

Synonyms:2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

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Chemical Property of 2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

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Technology Process of 2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

There total 4 articles about 2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1192165-07-3
N'-acetoxy-2-[4-(4-tert-butylphenyl)-2-oxopyridin-1(2H)-yl]ethanimidamide

: 1192165-17-5
2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

Guidance literature:: With hydrogen; acetic acid; 20% palladium hydroxide-activated charcoal; at 20 ℃; for 4h;

Reference yield:

: 942947-02-6
2-(benzyloxy)-4-(4-tert-butylphenyl)pyridine

: 1192165-17-5
2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 13 h / Reflux; Inert atmosphere

2: hydroxylamine / ethanol; water / 1 h / Reflux

3: triethylamine / 1,4-dioxane / 3 h / 20 °C

4: hydrogen; acetic acid / 20% palladium hydroxide-activated charcoal / 4 h / 20 °C

With hydrogen; hydroxylamine; acetic acid; triethylamine; 20% palladium hydroxide-activated charcoal; In 1,4-dioxane; ethanol; water; acetonitrile;

Reference yield:

: 1192165-08-4
2-[4-(4-tert-butylphenyl)-2-oxopyridin-1(2H)-yl]-N'-(hydroxy)ethanimidamide

: 1192165-17-5
2-[4-(4-tert-butylphenyl)-2-oxopiperidin-1-yl]ethanimidamide acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 3 h / 20 °C

2: hydrogen; acetic acid / 20% palladium hydroxide-activated charcoal / 4 h / 20 °C

With hydrogen; acetic acid; triethylamine; 20% palladium hydroxide-activated charcoal; In 1,4-dioxane;