13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene

Base Information

• Chemical Name: 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene
• CAS No.: 244217-92-3
• Molecular Formula: C₃₂H₄₆N₁₀
• Molecular Weight: 570.784

Synonyms:13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene

Chemical Property of 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene

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Technology Process of 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene

There total 4 articles about 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo-[22.2.1.111,14.02,6.015,19]-octacosa-1(27),9,11,14(28),22,24-hexaene → 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.111,14]-octacosa-1(27),11,14(28),24-tetraene (244217-92-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 2h;

DOI:10.1021/jo981699i

Reference yield: 83.0%

13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1(27),9,11,14(28),22,24-hexaene (244217-88-7) → 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.111,14]-octacosa-1(27),11,14(28),24-tetraene (244217-92-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 25 ℃; for 2h;

DOI:10.1021/jm2017144

Reference yield:

1-benzyl-3,5-pyrazoledicarbaldehyde (244217-84-3) → 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.111,14]-octacosa-1(27),11,14(28),24-tetraene (244217-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / acetonitrile / 25 °C

2: 86 percent / NaBH₄ / ethanol / 2 h / 20 °C

With sodium tetrahydroborate; In ethanol; acetonitrile; 1: Condensation / 2: Reduction;

DOI:10.1021/jo981699i

upstream raw materials:

1-benzyl-3,5-bis(hydroxymethyl)pyrazole

1-benzyl-3,5-pyrazoledicarbaldehyde

13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene

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