(E)-6-Benzyloxy-hex-3-enal

Base Information

Chemical Name:(E)-6-Benzyloxy-hex-3-enal
CAS No.:916323-73-4
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:(E)-6-Benzyloxy-hex-3-enal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-6-Benzyloxy-hex-3-enal

Chemical Property:

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Technology Process of (E)-6-Benzyloxy-hex-3-enal

There total 3 articles about (E)-6-Benzyloxy-hex-3-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 916323-73-4
(E)-6-Benzyloxy-hex-3-enal

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperidine; xylenes; Me₃SiCl / 136 °C

1.2: LiAlH₄ / tetrahydrofuran

2.1: Dess-Martin periodinane / CH₂Cl₂

With piperidine; chloro-trimethyl-silane; Dess-Martin periodane; xylenes; In dichloromethane; 1.1: Knoevenagel condensation / 2.1: Dess-Martin oxidation;
DOI:10.1039/b612697a

Reference yield:

: 174737-38-3
(3E)-6-(benzyloxy)-hex-3-en-1-ol

: 916323-73-4
(E)-6-Benzyloxy-hex-3-enal

Guidance literature:: With Dess-Martin periodane; In dichloromethane;
DOI:10.1039/b612697a

Reference yield:

: (E)-6-(benzyloxy)hex-3-enoic acid

: 916323-73-4
(E)-6-Benzyloxy-hex-3-enal

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1039/c2ob25100k