2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

Base Information

Chemical Name:2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside
CAS No.:242147-26-8
Molecular Formula:C₃₂H₃₈O₈
Molecular Weight:550.649
Hs Code.:

Synonyms:2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

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Chemical Property of 2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

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Technology Process of 2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

There total 4 articles about 2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 76-83-5
trityl chloride

: 242147-25-7
2-hydroxyethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

: 242147-26-8
2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

Guidance literature:: With pyridine; dmap; at 80 ℃; for 30h;
DOI:10.1080/07328309908544031

Reference yield:

: 140420-69-5
allyl α-D-xylopyranoside

: 242147-26-8
2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 46 percent / (+/-)-camphorsulfonic acid; (MeO)3CH / methanol / 1.5 h / Heating

2.1: ozone / CH₂Cl₂; methanol / 1.5 h / -70 °C

2.2: 98 percent / sodium borohydride / CH₂Cl₂; methanol / -70 - 20 °C

3.1: 71 percent / pyridine; DMAP / 30 h / 80 °C

With pyridine; dmap; camphor-10-sulfonic acid; ozone; trimethyl orthoformate; In methanol; dichloromethane; 1.1: ketalization / 2.1: ozonolysis / 2.2: Reduction / 3.1: Etherification;
DOI:10.1080/07328309908544031

Reference yield:

: 176798-33-7
2,2,3,3-tetramethoxybutane

: 242147-26-8
2-(trityloxy)ethyl 3,4-O-[(2S,3S)-2,3-dimethoxybutane-2,3-diyl]-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 46 percent / (+/-)-camphorsulfonic acid; (MeO)3CH / methanol / 1.5 h / Heating

2.1: ozone / CH₂Cl₂; methanol / 1.5 h / -70 °C

2.2: 98 percent / sodium borohydride / CH₂Cl₂; methanol / -70 - 20 °C

3.1: 71 percent / pyridine; DMAP / 30 h / 80 °C

With pyridine; dmap; camphor-10-sulfonic acid; ozone; trimethyl orthoformate; In methanol; dichloromethane; 1.1: ketalization / 2.1: ozonolysis / 2.2: Reduction / 3.1: Etherification;
DOI:10.1080/07328309908544031