(2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

Base Information

Chemical Name:(2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate
CAS No.:1370411-71-4
Molecular Formula:C₂₅H₂₈O₇
Molecular Weight:440.493
Hs Code.:

Synonyms:(2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

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Chemical Property of (2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

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Technology Process of (2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

There total 1 articles about (2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₄O₅

: 108-24-7
acetic anhydride

: 1370411-71-4
(2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

: 1370411-88-3
(2R,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

Guidance literature:: With pyridine; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo300554w

Reference yield: 98.0%

: 26661-13-2
4-N-benzoylcytosine

: 1370411-71-4
(2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

: 1370411-73-6
(3'S,5'R)-N4-benzoyl-1-(2'-acetoxy-3',5'-O-dibenzyl-3',5'-ethano-β-D-ribofuranosyl)cytidine

Guidance literature:: 4-N-benzoylcytosine; (2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;

With tin(IV) chloride; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo300554w

Reference yield: 73.0%

: 1370411-71-4
(2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate

: 65-71-4,28806-14-6,691841-57-3
thymin

: 1370411-72-5
(3'S,5'R)-1-(2'-acetoxy-3',5'-O-dibenzyl-3',5'-ethano-β-D-ribofuranosyl)thymidine

Guidance literature:: (2S,3R,3aR,6R,6aR)-3a,6-bis(benzyloxy)-2-(acetyloxy)-hexahydro-2H-cyclopenta[b]furan-3-yl acetate; thymin; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 80 ℃; for 1h; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 50 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo300554w