(methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

Base Information

Chemical Name:(methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone
CAS No.:101696-49-5
Molecular Formula:C₂₀H₂₆O₈
Molecular Weight:394.422
Hs Code.:

Synonyms:(methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

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Chemical Property of (methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

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Technology Process of (methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

There total 5 articles about (methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 116261-35-9
(3R,5R)-3-(4-Methoxy-benzyloxy)-5-((3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-tetrahydro-furan-2-ol

: 101696-49-5
(methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

Guidance literature:: With silver(III) oxide; In xylene;
DOI:10.1021/ja00269a080

Reference yield:

: 33985-40-9
(3aR,4S,6R,6aR)-tetrahydro-6-methoxy-2,2-dimethylfuro-[3,4-d][1,3]dioxole-4-carbaldehyde

: 101696-49-5
(methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent

2: NaBH₄-CeCl₃ / methanol

3: NaH

4: 1.) NaIO₄; 2.) K₂CO₃ / 1.) OsO₄ / 2.) MeOH, r.t

5: 86 percent / Ag₂O₃-Celite / xylene

With sodium tetrahydroborate; sodium periodate; cerium(III) chloride; silver(III) oxide; sodium hydride; potassium carbonate; osmium(VIII) oxide; In methanol; xylene;
DOI:10.1021/ja00269a080

Reference yield:

: 99441-05-1
methyl 5,9-anhydro-6,8-dideoxy-2,3-O-(1-methylethylidene)-β-D-allo-non-8-enofuranosid-7-ulose

: 101696-49-5
(methyl 6-deoxy-7-O-<(4-methoxyphenyl)methyl>-2,3-O-(1-methylethylidene)-L-glycero-β-D-allo-octafuranosid)uronic acid α-lactone

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄-CeCl₃ / methanol

2: NaH

3: 1.) NaIO₄; 2.) K₂CO₃ / 1.) OsO₄ / 2.) MeOH, r.t

4: 86 percent / Ag₂O₃-Celite / xylene

With sodium tetrahydroborate; sodium periodate; cerium(III) chloride; silver(III) oxide; sodium hydride; potassium carbonate; osmium(VIII) oxide; In methanol; xylene;
DOI:10.1021/ja00269a080