C₄₄H₅₉ClN₂O₇

Base Information

Chemical Name:C₄₄H₅₉ClN₂O₇
CAS No.:1449796-63-7
Molecular Formula:C₄₄H₅₉ClN₂O₇
Molecular Weight:763.415
Hs Code.:

C<sub>44</sub>H<sub>59</sub>ClN<sub>2</sub>O<sub>7</sub>

Synonyms:C₄₄H₅₉ClN₂O₇

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Chemical Property of C₄₄H₅₉ClN₂O₇

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Technology Process of C₄₄H₅₉ClN₂O₇

There total 16 articles about C₄₄H₅₉ClN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1449797-81-2
C₄₈H₆₇ClN₂O₇

: 1449796-63-7
C₄₄H₅₉ClN₂O₇

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1449797-75-4
C₄₀H₅₃ClN₂O₆

: 1449796-63-7
C₄₄H₅₉ClN₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1: N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride / dichloromethane / 3 h / 20 °C

2: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 0 °C

3: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

4: triethylamine; dmap / dichloromethane / 1 h / 0 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

6: potassium hydroxide / toluene; ethanol / 1 h / 20 °C

7: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

With methanol; dmap; sodium tetrahydroborate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene;

Reference yield:

: 1422356-82-8
C₃₃H₄₉NO₆

: 1449796-63-7
C₄₄H₅₉ClN₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1: acetic acid; sodium nitrite / dimethyl sulfoxide / 20 °C

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

3: N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride / dichloromethane / 3 h / 20 °C

4: sodium tetrahydroborate; methanol / tetrahydrofuran / 0.5 h / 0 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

6: triethylamine; dmap / dichloromethane / 1 h / 0 °C

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

8: potassium hydroxide / toluene; ethanol / 1 h / 20 °C

9: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

With methanol; dmap; sodium tetrahydroborate; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium hydroxide; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;