(S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate
CAS No.:1367878-32-7
Molecular Formula:C₂₂H₃₆N₃O₅P
Molecular Weight:453.519
Hs Code.:

Synonyms:(S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate

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Chemical Property of (S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate

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Technology Process of (S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate

There total 1 articles about (S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 479423-37-5
tert-butyl 2-methylbenzylidenecarbamate

: 1367878-23-6
di-tert-butyl diazomethylphosphonate

: 1367878-32-7
(S)-tert-butyl 2-(di-tert-butoxyphosphoryl)-2-diazo-1-o-tolylethylcarbamate

Guidance literature:: With (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid; In toluene; at -40 ℃; for 6h; optical yield given as %ee; enantioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol300664d