C₄₉H₅₈N₆O₁₁

Base Information

Chemical Name:C₄₉H₅₈N₆O₁₁
CAS No.:1343407-40-8
Molecular Formula:C₄₉H₅₈N₆O₁₁
Molecular Weight:907.033
Hs Code.:

C<sub>49</sub>H<sub>58</sub>N<sub>6</sub>O<sub>11</sub>

Synonyms:C₄₉H₅₈N₆O₁₁

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Chemical Property of C₄₉H₅₈N₆O₁₁

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Technology Process of C₄₉H₅₈N₆O₁₁

There total 16 articles about C₄₉H₅₈N₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1343407-39-5
C₅₃H₆₂N₆O₁₃

: 1343407-40-8
C₄₉H₅₈N₆O₁₁

Guidance literature:: With pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 20 ℃; for 0.75h; Inert atmosphere;

Reference yield:

: C₁₅H₁₈N₂O₈

: 1343407-40-8
C₄₉H₅₈N₆O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

4.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

5.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

6.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

6.2: 20 - 65 °C

7.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane / 6.5 h / 20 °C

9.1: pyrrolidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

With pyrrolidine; 2,6-dimethylpyridine; lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; trichloroisocyanuric acid; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 3.1: Suzuki Coupling;

Reference yield:

: 1343407-33-9
C₂₂H₂₂N₂O₈

: 1343407-40-8
C₄₉H₅₈N₆O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

2.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

3.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

3.2: 20 - 65 °C

4.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 6.5 h / 20 °C

6.1: pyrrolidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

With pyrrolidine; lithium borohydride; ethanol; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;