1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

Base Information

Chemical Name:1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline
CAS No.:123042-38-6
Molecular Formula:C₂₇H₃₃N₃O₆
Molecular Weight:495.576
Hs Code.:

Synonyms:1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

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Chemical Property of 1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

Chemical Property:

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Technology Process of 1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

There total 4 articles about 1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 21691-43-0
(R,S)-2-(N-benzyloxycarbonylamino)pentanoic acid

: 85071-60-9
1-aminomethyl-5,7,8-trimethoxy-6-methylisoquinoline dihydrochloride

: 123042-38-6
1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In chloroform; at 0 ℃; for 0.25h;

Reference yield:

: 86433-67-2
5,7,8-trimethoxy-6-methyl-isoquinoline

: 123042-38-6
1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / 80percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

2: 96 percent / benzoyl chloride / H₂O / 0.5 h / Ambient temperature

3: 100 percent / cc. HCl, hydrogen / 10percent palladium on carbon / methanol / 2 h / 760 Torr

4: 84 percent / triethylamine, DCC / CHCl₃ / 0.25 h / 0 °C

With hydrogenchloride; hydrogen; benzoyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; chloroform; water;

Reference yield:

: 84018-50-8
6-methyl-5,7,8-trimethoxy-1-isoquinolinecarbonitrile

: 123042-38-6
1-(N-carbobenzyloxy-DL-norvalylaminomethyl)-5,7,8-trimethoxy-6-methylisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / cc. HCl, hydrogen / 10percent palladium on carbon / methanol / 2 h / 760 Torr

2: 84 percent / triethylamine, DCC / CHCl₃ / 0.25 h / 0 °C

With hydrogenchloride; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; chloroform;