2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Base Information

Chemical Name:2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene
CAS No.:929803-64-5
Molecular Formula:C₈₀H₁₀₄I₂O₆
Molecular Weight:1415.51
Hs Code.:

Synonyms:2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Suppliers and Price of 2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

There total 8 articles about 2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 13064-64-7
2,5-diiodo-1,4-hydroquinone

: 213680-85-4
1,3-bis{[3,5-bis(tert-butyl)benzyl]oxy}-5-(bromomethyl)benzene

: 929803-64-5
2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h;
DOI:10.1021/ol062793l

Reference yield:

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 929803-64-5
2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran / 4 h / 20 °C

3: 81 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

4: 78 percent / potassium carbonate / dimethylformamide / 4 h / 50 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol062793l

Reference yield:

: 916226-09-0
2,5-bis(methoxymethoxy)-1,4-diiodobenzene

: 929803-64-5
2,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / aq. HCl; methanol / 4 h / Heating

2: 78 percent / potassium carbonate / dimethylformamide / 4 h / 50 °C

With hydrogenchloride; methanol; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ol062793l