3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

Base Information

Chemical Name:3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide
CAS No.:184241-27-8
Molecular Formula:C₂₉H₄₅N₃O₇Si₂
Molecular Weight:603.863
Hs Code.:

Synonyms:3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

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Chemical Property of 3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

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Technology Process of 3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

There total 9 articles about 3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 17280-41-0
anti-pyruvic aldehyde 1-oxime

: 184241-23-4
Benzoic acid (2S,3S,3aR,9aR)-2-((S)-amino-cyano-methyl)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yl ester

: 184241-27-8
3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

Guidance literature:: With pyridine hydrochloride; In chloroform; Heating;
DOI:10.1002/hlca.19960790710

Reference yield:

: 184241-18-7
[Cyano-((2S,3S,3aS,9aR)-3-hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-methyl]-carbamic acid benzyl ester

: 184241-27-8
3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h / Ambient temperature

2: 19 percent / H₂ / Pd/C / tetrahydrofuran; methanol

3: pyridine hydrochloride / CHCl₃

With pyridine; hydrogen; pyridine hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1002/hlca.19960790710

Reference yield:

: 184241-20-1
2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

: 184241-27-8
3-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-5-methylpyrazin-2-amine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / H₂ / Pd/C / tetrahydrofuran; methanol

2: pyridine hydrochloride / CHCl₃

With hydrogen; pyridine hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1002/hlca.19960790710