1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene

Base Information

• Chemical Name: 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene
• CAS No.: 1586038-80-3
• Molecular Formula: C₂₆H₁₆F₆O₂S
• Molecular Weight: 506.468

Synonyms:1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene

Chemical Property of 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene

There total 7 articles about 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-1,3-dioxolane-phenyl)-3-thienyl]perfluorocyclopentene (1427283-27-9) → 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene (1586038-80-3)

Guidance literature:

With pyridine; toluene-4-sulfonic acid; In water; acetone; at 59.84 ℃;

DOI:10.1002/poc.3257

Reference yield:

4-(4-bromo-5-methylthiophen-2-yl)benzaldehyde (550348-56-6) → 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene (1586038-80-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / benzene / Dean-Stark; Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78.16 °C / Inert atmosphere

2.2: 2 h / -78.16 °C / Inert atmosphere

3.1: pyridine; toluene-4-sulfonic acid / acetone; water / 59.84 °C

With pyridine; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; water; acetone; benzene;

DOI:10.1002/poc.3257

Reference yield:

3-bromo-5-(4-(1,3-dioxolan-2-yl)phenyl)-2-methylthiophene (550348-57-7) → 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene (1586038-80-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78.16 °C / Inert atmosphere

1.2: 2 h / -78.16 °C / Inert atmosphere

2.1: pyridine; toluene-4-sulfonic acid / acetone; water / 59.84 °C

With pyridine; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; water; acetone;

DOI:10.1002/poc.3257

upstream raw materials:

4-(4-bromo-5-methylthiophen-2-yl)benzaldehyde

3-bromo-5-(4-(1,3-dioxolan-2-yl)phenyl)-2-methylthiophene

octaperfluorocyclopentene

3-bromo-2-methyl-1-benzofuran

Downstream raw materials:

C₂₆H₁₆F₆O₂S

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1586038-80-3 1-(2-methyl-1-benzofuran-3-yl)-2-[2-methyl-5-(4-benzaldehyde)-3-thienyl]perfluorocyclopentene

Send

Send

Metric Ton KG G Pound L ML

Send

Send