(E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

Base Information

Chemical Name:(E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine
CAS No.:1222085-52-0
Molecular Formula:C₂₃H₃₆BNO₃
Molecular Weight:385.355
Hs Code.:

Synonyms:(E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

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Chemical Property of (E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

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Technology Process of (E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

There total 4 articles about (E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 110-91-8,99108-56-2
morpholine

: 1222085-35-9
(E)-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-enyl acetate

: 1222085-52-0
(E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

Guidance literature:: With Pd(OAc)2; PPh₃; In tetrahydrofuran; (Ph)CH(OAc)C(CH(nBu))B(pin) (80% ee) combined with Pd and PPh3 catalyst,HNC4H8O, reacted at room temp. for 12 h; 80% ee;
DOI:10.1002/anie.200905399

Reference yield: 45.0%

: 110-91-8,99108-56-2
morpholine

: 1222085-37-1
(E)-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-1-en-3-yl acetate

: 1222085-52-0
(E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

Guidance literature:: (E)-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-1-en-3-yl acetate; With palladium diacetate; triphenylphosphine; In tetrahydrofuran; Inert atmosphere;

morpholine; In tetrahydrofuran; at 20 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1002/anie.200905399

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 1222085-35-9
(E)-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-enyl acetate

: C₂₃H₃₆BNO₃

: 1222085-52-0
(E)-4-(1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-en-1-yl)morpholine

Guidance literature:: (E)-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hept-2-enyl acetate; With palladium diacetate; triphenylphosphine; In tetrahydrofuran; Inert atmosphere;

morpholine; In tetrahydrofuran; at 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200905399