C₁₄H₂₁Cl₃Si

Base Information

• Chemical Name: C₁₄H₂₁Cl₃Si
• CAS No.: 1252913-95-3
• Molecular Formula: C₁₄H₂₁Cl₃Si
• Molecular Weight: 323.765
• Mol file: 1252913-95-3.mol

Synonyms:C₁₄H₂₁Cl₃Si

Chemical Property of C₁₄H₂₁Cl₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₁Cl₃Si

There total 4 articles about C₁₄H₂₁Cl₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H22Cl2OSi (1252914-19-4) → C14H20Cl2Si + C14H21Cl3Si (1252913-95-3)

Guidance literature:

With pyridine; thionyl chloride; In benzene; at 0 ℃; for 2h;

DOI:10.1002/poc.1667

Reference yield:

C9H11Cl3Si (85491-22-1) → C14H20Cl2Si + C14H21Cl3Si (1252913-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: magnesium / diethyl ether

1.2: 3 h / 0 - 20 °C

2.1: pyridine; thionyl chloride / benzene / 2 h / 0 °C

With pyridine; thionyl chloride; magnesium; In diethyl ether; benzene; 1.2: Grignard reaction;

DOI:10.1002/poc.1667

Reference yield:

1-bromo-3,5-dichlorobenzene (19752-55-7) → C14H20Cl2Si + C14H21Cl3Si (1252913-95-3)

Guidance literature:

Multi-step reaction with 3 steps

2.1: magnesium / diethyl ether

2.2: 3 h / 0 - 20 °C

3.1: pyridine; thionyl chloride / benzene / 2 h / 0 °C

With pyridine; thionyl chloride; magnesium; In diethyl ether; benzene; 1.1: Grignard reaction / 2.2: Grignard reaction;

DOI:10.1002/poc.1667

upstream raw materials:

C₁₄H₂₂Cl₂OSi

C₉H₁₁Cl₃Si

1-bromo-3,5-dichlorobenzene

pivalaldehyde

Downstream raw materials:

tert-butylethylene