(1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

Base Information

Chemical Name:(1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol
CAS No.:455330-54-8
Molecular Formula:C₂₃H₃₁N₃O₂Si
Molecular Weight:409.604
Hs Code.:

Synonyms:(1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

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Chemical Property of (1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

Chemical Property:

Purity/Quality:

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Technology Process of (1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

There total 8 articles about (1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 455330-44-6
Methanesulfonic acid (1S,2S,4R)-2-(tert-butyl-diphenyl-silanyloxymethyl)-4-hydroxy-cyclohexyl ester

: 455330-54-8
(1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide;

Reference yield:

: 96894-00-7
(1S,2S)-4,4-ethylenedioxy-2-hydroxymethylcyclohexanol

: 455330-54-8
(1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / imidazole; DMAP / dimethylformamide

2: 100 percent / aq. acetic acid / dimethylformamide

3: 92 percent / DMAP / pyridine

4: 86 percent / sodium borohydride / methanol

5: 95 percent / sodium azide / dimethylformamide

With 1H-imidazole; dmap; sodium tetrahydroborate; sodium azide; acetic acid; In pyridine; methanol; N,N-dimethyl-formamide;

Reference yield:

: 96893-99-1
(1R,2S)-5,5-(Ethylendioxy)-2-hydroxycyclohexancarbonsaeure-ethylester

: 455330-54-8
(1R,3R,4R)-4-Azido-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohexanol

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / DMAP / pyridine

2: 99 percent / lithium aluminum hydride / diethyl ether

3: 84 percent / imidazole; DMAP / dimethylformamide

4: 100 percent / aq. acetic acid / dimethylformamide

5: 92 percent / DMAP / pyridine

6: 86 percent / sodium borohydride / methanol

7: 95 percent / sodium azide / dimethylformamide

With 1H-imidazole; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium azide; acetic acid; In pyridine; methanol; diethyl ether; N,N-dimethyl-formamide;