(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Base Information

Chemical Name:(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester
CAS No.:882429-54-1
Molecular Formula:C₄₈H₆₂O₉
Molecular Weight:783.015
Hs Code.:

(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Synonyms:(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Suppliers and Price of (E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

There total 5 articles about (E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59860-28-5
fusidic acid pivaloyloxymethyl ester

: 882429-54-1
(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 64 percent / O₃ / CH₂Cl₂ / -78 °C

2.1: t-BuOK / toluene / 0.25 h / Heating

2.2: toluene / 0.25 h / Heating

With potassium tert-butylate; ozone; In dichloromethane; toluene; 2.2: Wittig reaction;
DOI:10.1021/jm050583t

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 882429-54-1
(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / Et₃N / dimethylformamide

2.1: 64 percent / O₃ / CH₂Cl₂ / -78 °C

3.1: t-BuOK / toluene / 0.25 h / Heating

3.2: toluene / 0.25 h / Heating

With potassium tert-butylate; ozone; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3.2: Wittig reaction;
DOI:10.1021/jm050583t

Reference yield:

: 3482-49-3,4680-36-8,6990-06-3,19030-42-3,107380-53-0
fusidine

: 882429-54-1
(E)-2-[(3R,4S,5S,8S,9S,10S,11R,13R,14S,16S)-16-Acetoxy-3,11-dihydroxy-4,8,10,14-tetramethyl-hexadecahydro-cyclopenta[a]phenanthren-(17Z)-ylidene]-6-(4-benzoyl-phenyl)-hex-5-enoic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / Et₃N / dimethylformamide

2.1: 64 percent / O₃ / CH₂Cl₂ / -78 °C

3.1: t-BuOK / toluene / 0.25 h / Heating

3.2: toluene / 0.25 h / Heating

With potassium tert-butylate; ozone; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3.2: Wittig reaction;
DOI:10.1021/jm050583t