acetic acid (1R,2S,3R,4S,6R)-2,3-diacetoxy-6-acetoxymethyl-4-acetylaminocyclohexyl ester

Base Information

Chemical Name:acetic acid (1R,2S,3R,4S,6R)-2,3-diacetoxy-6-acetoxymethyl-4-acetylaminocyclohexyl ester
CAS No.:132342-13-3
Molecular Formula:C₁₇H₂₅NO₉
Molecular Weight:387.387
Hs Code.:

Synonyms:acetic acid (1R,2S,3R,4S,6R)-2,3-diacetoxy-6-acetoxymethyl-4-acetylaminocyclohexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetic acid (1R,2S,3R,4S,6R)-2,3-diacetoxy-6-acetoxymethyl-4-acetylaminocyclohexyl ester

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Technology Process of acetic acid (1R,2S,3R,4S,6R)-2,3-diacetoxy-6-acetoxymethyl-4-acetylaminocyclohexyl ester

There total 32 articles about acetic acid (1R,2S,3R,4S,6R)-2,3-diacetoxy-6-acetoxymethyl-4-acetylaminocyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 108-24-7
acetic anhydride

: DL-5a-carba-α-mannopyranosylamine

: 64589-26-0,68108-50-9,73651-28-2,74561-05-0,87038-27-5,108866-25-7,132342-13-3
1α,2β,3β-(triacetoxy)-4α-acetamido-6β-(acetoxymethyl)-1,2,3-cyclohexanetriol

Guidance literature:: With pyridine; for 6h; Ambient temperature;
DOI:10.1016/S0040-4039(98)01610-4

Reference yield: 71.0%

: (1RS,4SR,6RS)-2,3-epoxy-6-(hydroxymethyl)-4-(tosylamino)cyclohexane-1-ol

: 108-24-7
acetic anhydride

: (+/-)-2-epi-3-epi-validamine pentaacetate

: 64589-26-0,68108-50-9,73651-28-2,74561-05-0,87038-27-5,108866-25-7,132342-13-3
(+/-)-<(1,3/2,4,5)-5-acetamido-2,3,4-triacetoxycyclohexyl>-methyl acetate

Guidance literature:: (1RS,4SR,6RS)-2,3-epoxy-6-(hydroxymethyl)-4-(tosylamino)cyclohexane-1-ol; With sulfuric acid; In methanol; at 20 ℃; for 12h;

With sodium; In ammonia; at -78 ℃; for 0.333333h;

acetic anhydride; With pyridine; Further stages.;
DOI:10.3987/COM-06-10887