(C₅H₅)Mo₂(CO)6(C₅H₄C₄H₇O)

Base Information

• Chemical Name: (C₅H₅)Mo₂(CO)6(C₅H₄C₄H₇O)
• CAS No.: 113753-77-8
• Molecular Formula: C₂₀H₁₆Mo₂O₇
• Molecular Weight: 560.223
• Mol file: 113753-77-8.mol

Synonyms:(C₅H₅)Mo₂(CO)6(C₅H₄C₄H₇O)

Chemical Property of (C₅H₅)Mo₂(CO)6(C₅H₄C₄H₇O)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (C₅H₅)Mo₂(CO)6(C₅H₄C₄H₇O)

There total 1 articles about (C₅H₅)Mo₂(CO)6(C₅H₄C₄H₇O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

Na[CpMo(CO)3] (12107-35-6) → ((C5H5)Mo(CO)3)2 (12091-64-4) + (η5-cyclopentadienyl)MoCl(CO)3 + (C5H5)Mo2(CO)6(C5H4C4H7O) (113753-77-8)

Guidance literature:

With tetrahydrofuran; thionyl chloride; In tetrahydrofuran; THF soln. of SOCl2 was added dropwise (15 min) to a stirred soln. of CpMo(CO)3Na in THF at -97°C under nitrogen atmosphere; evapd., residue was extd. with Et2O, chromd. on a SiO2 column (eluent Et2O-light petroleum, then Et2O); (CpMo(CO)3)2 was identified by IR and (1)H NMR spectra, elem. anal. for CpMoCl(CO)3 and THF-substituted dimer (crystd. from Et2O-petroleum ether);

upstream raw materials:

Na[CpMo(CO)3]