C₂₂H₂₉NO₃

Base Information Edit

Chemical Name:C₂₂H₂₉NO₃
CAS No.:1185253-10-4
Molecular Formula:C₂₂H₂₉NO₃
Molecular Weight:355.477
Hs Code.:
Mol file:1185253-10-4.mol

C<sub>22</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₂H₂₉NO₃

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Chemical Property of C₂₂H₂₉NO₃ Edit

Chemical Property:

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Technology Process of C₂₂H₂₉NO₃

There total 5 articles about C₂₂H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 254438-52-3
C₂₆H₃₇NO₃

: 1185253-10-4
C₂₂H₂₉NO₃

Guidance literature:: C₂₆H₃₇NO₃; With trifluoroacetic acid; In toluene; at 50 ℃; for 25.5h; Industry scale;

With sodium hydroxide; In water; toluene; at 15 - 20 ℃; pH=5 - 6; Industry scale;

Reference yield:

: 110-62-3
pentanal

: 1185253-10-4
C₂₂H₂₉NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 60 h / 5 - 35 °C / Industry scale

1.2: 30 °C / Industry scale

2.1: sulfuric acid / n-heptane / 18 h / 19 - 25 °C / Industry scale; Sealed vessel

3.1: n-hexyllithium / n-heptane; tetrahydrofuran / 0.5 h / -65 - -55 °C / Industry scale

3.2: 1.5 h / -65 - -55 °C / Industry scale

4.1: (1S)-(+)-(10-camphorsulfonyl)-oxaziridine / n-heptane; tetrahydrofuran / 6 h / -65 - -55 °C / Industry scale

4.2: -60 - -40 °C / Industry scale

5.1: trifluoroacetic acid / toluene / 25.5 h / 50 °C / Industry scale

5.2: 15 - 20 °C / pH 5 - 6 / Industry scale

With pyridine; n-hexyllithium; (1S)-(+)-(10-camphorsulfonyl)-oxaziridine; trifluoroacetic acid; sulfuric acid; In tetrahydrofuran; n-heptane; toluene;

Reference yield:

: 18999-28-5
3-(n-Butyl)acrylic acid

: 1185253-10-4
C₂₂H₂₉NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / n-heptane / 18 h / 19 - 25 °C / Industry scale; Sealed vessel

2.1: n-hexyllithium / n-heptane; tetrahydrofuran / 0.5 h / -65 - -55 °C / Industry scale

2.2: 1.5 h / -65 - -55 °C / Industry scale

3.1: (1S)-(+)-(10-camphorsulfonyl)-oxaziridine / n-heptane; tetrahydrofuran / 6 h / -65 - -55 °C / Industry scale

3.2: -60 - -40 °C / Industry scale

4.1: trifluoroacetic acid / toluene / 25.5 h / 50 °C / Industry scale

4.2: 15 - 20 °C / pH 5 - 6 / Industry scale

With n-hexyllithium; (1S)-(+)-(10-camphorsulfonyl)-oxaziridine; trifluoroacetic acid; sulfuric acid; In tetrahydrofuran; n-heptane; toluene;