(S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid

Base Information

• Chemical Name: (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid
• CAS No.: 214853-74-4
• Molecular Formula: C₁₅H₂₂O₂
• Molecular Weight: 234.338

Synonyms:(S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid

Chemical Property of (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid

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Technology Process of (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid

There total 1 articles about (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Propionic acid (1S,5R)-5-isopropenyl-2-methyl-1-vinyl-cyclohex-2-enyl ester (214853-72-2) → (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid (214853-74-4) + (R)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid

Guidance literature:

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; Title compound not separated from byproducts.;

DOI:10.1021/jo010752r

Reference yield: 74.0%

(S)-1-phenyl-ethylamine (2627-86-3) + (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-butyric acid (214853-74-4) → (S)-4-[(R)-5-Isopropenyl-2-methyl-cyclohex-2-en-(E)-ylidene]-2-methyl-N-((S)-1-phenyl-ethyl)-butyramide

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1021/jo010752r

upstream raw materials:

Propionic acid (1S,5R)-5-isopropenyl-2-methyl-1-vinyl-cyclohex-2-enyl ester

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