(R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Base Information

Chemical Name:(R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol
CAS No.:464195-29-7
Molecular Formula:C₁₆H₂₄O₅S
Molecular Weight:328.43
Hs Code.:

Synonyms:(R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Suppliers and Price of (R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

There total 4 articles about (R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 464195-28-6
(3R)-1-(4-methylbenzenesulfonate)-4,4-dimethyl-1,3-pentanediol

: 464195-29-7
(R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Guidance literature:: With dmap; triethylamine; Yield given;
DOI:10.1016/S0040-4039(97)01580-3

Reference yield:

: 158724-91-5
(R)-4,4-dimethyl-1,3-pentanediol

: 464195-29-7
(R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / DMAP; pyridine / CH₂Cl₂ / 0 - 20 °C

2: DMAP; Et₃N / CH₂Cl₂ / 5 h / 20 °C

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1021/jo010880f

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 464195-29-7
(R,R)-4,4-dimethyl-3-acetate 1-(4-methylbenzenesulfonate)-1,3-pentanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / DMAP; pyridine / CH₂Cl₂ / 0 - 20 °C

2: DMAP; Et₃N / CH₂Cl₂ / 5 h / 20 °C

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1021/jo010880f