(+/-)-3,5-dinitro-o-tyrosine

Base Information

• Chemical Name: (+/-)-3,5-dinitro-o-tyrosine
• CAS No.: 203568-96-1
• Molecular Formula: C₉H₉N₃O₇
• Molecular Weight: 271.186

Synonyms:(+/-)-3,5-dinitro-o-tyrosine

Chemical Property of (+/-)-3,5-dinitro-o-tyrosine

Chemical Property:

Purity/Quality:

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Technology Process of (+/-)-3,5-dinitro-o-tyrosine

There total 1 articles about (+/-)-3,5-dinitro-o-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroxy-phenylalanine (709-16-0,2370-61-8,7423-92-9,24008-77-3) → (+/-)-3,5-dinitro-o-tyrosine (203568-96-1)

Guidance literature:

With nitronium tetrafluoborate; In acetonitrile; for 8h;

DOI:10.1021/jm950028z

Reference yield: 98.0%

acetic anhydride (108-24-7) + (+/-)-3,5-dinitro-o-tyrosine (203568-96-1) → (R,S)-N-acetyl-3,5-dinitro-o-tyrosine

Guidance literature:

With sodium hydroxide; In water; for 0.666667h; Ambient temperature;

DOI:10.1021/jm970276q

Reference yield: 96.0%

di-tert-butyl dicarbonate (24424-99-5) + (+/-)-3,5-dinitro-o-tyrosine (203568-96-1) → (R,S)-N-(tert-butoxycarbonyl)-3,5-dinitro-o-tyrosine (203569-02-2)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jm970276q

upstream raw materials:

2-hydroxy-phenylalanine

Downstream raw materials:

(R,S)-N-(tert-butoxycarbonyl)-3,5-dinitro-o-tyrosine

N-(tert-butoxycarbonyl)-β-(3,5-dinitro-2-methoxyphenyl)-α-alanine

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