1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil

Base Information

• Chemical Name: 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil
• CAS No.: 129928-67-2
• Molecular Formula: C₂₉H₂₈N₄O₅
• Molecular Weight: 512.565

Synonyms:1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil

Chemical Property of 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil

Chemical Property:

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Technology Process of 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil

There total 1 articles about 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.1%

1-{(2R,5R)-4-Benzeneselenonyl-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-2,5-dihydro-furan-2-yl}-1H-pyrimidine-2,4-dione (125417-96-1) → 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-β-D-glycero-pent-2'-eno-furanosyl)uracil (129928-66-1) + 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2'-ulose hydrazone-β-D-erythro-pentofuranosyl)uracil (129928-67-2) + 1-(5'-O-(4-monomethoxytrityl)-2',3'-dideoxy-2',3'-biimino-β-D-ribofuranosyl)uracil (129928-65-0)

Guidance literature:

With hydrazine; In tetrahydrofuran; at 40 ℃; for 2h;

DOI:10.1016/S0040-4020(01)88395-2

upstream raw materials:

1-{(2R,5R)-4-Benzeneselenonyl-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-2,5-dihydro-furan-2-yl}-1H-pyrimidine-2,4-dione

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