Technology Process of 2-imidazolyl cyclohexanone
There total 4 articles about 2-imidazolyl cyclohexanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 40 - 80 ℃;
for 21h;
Inert atmosphere;
DOI:10.1021/acs.orglett.6b03334
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 76 percent / ethanol / 70 h / Heating
2: 1.) trifluoroacetic anhydride, dimethyl sulfoxide, 2.) triethylamine / 1.) CH2Cl2, room temperature, 2 h, 2.) from -65 deg C to 0 deg C, 1 h
With
dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
ethanol;
DOI:10.3987/COM-89-5280
- Guidance literature:
-
With
dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
Yield given. Multistep reaction;
1.) CH2Cl2, room temperature, 2 h, 2.) from -65 deg C to 0 deg C, 1 h;
DOI:10.3987/COM-89-5280
