[(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3

Base Information

Chemical Name:[(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3
CAS No.:86497-28-1
Molecular Formula:C₂H₄Cl₂*C₂₉H₃₂NO₄PRe*F₆P
Molecular Weight:919.682
Hs Code.:

Synonyms:[(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3

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Chemical Property of [(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3

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Technology Process of [(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3

There total 1 articles about [(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 86497-35-0
(η-C5Me5)Re(NO)(P(OPh)3)(CH3)

: 437-17-2
tritylium hexafluorophosphate

: 86497-28-1
[(η-C5Me5)Re(NO)(PPh3)(=CH2)]+PF6-*CHCl2CH3

Guidance literature:: In further solvent(s); complex in CHCl2CH3 was treated with CPh3PF6 at -78°C for 2 h, N2 atm.; evapn. in vac., suspending in benzene, filtration, washing with benzeneand hexane, recrystn. (CHCl2CH3/hexane);
DOI:10.1021/ja00356a018