C₃₇H₅₆O₁₀

Base Information

Chemical Name:C₃₇H₅₆O₁₀
CAS No.:1450842-84-8
Molecular Formula:C₃₇H₅₆O₁₀
Molecular Weight:660.846
Hs Code.:

C<sub>37</sub>H<sub>56</sub>O<sub>10</sub>

Synonyms:C₃₇H₅₆O₁₀

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Chemical Property of C₃₇H₅₆O₁₀

Chemical Property:

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Technology Process of C₃₇H₅₆O₁₀

There total 7 articles about C₃₇H₅₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1450842-80-4
C₂₉H₄₂O₆

: 1332478-35-9
C₁₄H₂₀O₄S

: 1450842-82-6
C₃₇H₅₆O₁₀

: 1450842-84-8
C₃₇H₅₆O₁₀

Guidance literature:: C₂₉H₄₂O₆; C₁₄H₂₀O₄S; With 2,6-di-tert-butyl-4-methyl-phenol; In diethyl ether; at 20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere;

With methyl trifluoromethanesulfonate; In diethyl ether; at 25 ℃; for 96h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol402095g

Reference yield:

: 1450842-65-5
C₁₆H₃₂O₃Si

: 1450842-82-6
C₃₇H₅₆O₁₀

: 1450842-84-8
C₃₇H₅₆O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 °C / Inert atmosphere

1.3: 2 h / -78 - 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 4 h / -78 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 1 h / -40 - -20 °C / Inert atmosphere

5.1: 2,6-di-tert-butyl-4-methyl-phenol / diethyl ether / 0.33 h / 20 °C / Molecular sieve; Inert atmosphere

5.2: 96 h / 25 °C / Molecular sieve; Inert atmosphere

With sodium tetrahydroborate; 2,6-di-tert-butyl-4-methyl-phenol; diethyl methoxy borane; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol402095g

Reference yield:

: 1450842-64-4
C₁₆H₃₄O₃Si

: 1450842-82-6
C₃₇H₅₆O₁₀

: 1450842-84-8
C₃₇H₅₆O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 4 h / -78 °C / Inert atmosphere

2.1: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 1 h / -40 - -20 °C / Inert atmosphere

4.1: 2,6-di-tert-butyl-4-methyl-phenol / diethyl ether / 0.33 h / 20 °C / Molecular sieve; Inert atmosphere

4.2: 96 h / 25 °C / Molecular sieve; Inert atmosphere

With sodium tetrahydroborate; 2,6-di-tert-butyl-4-methyl-phenol; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol402095g