1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

Base Information

Chemical Name:1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone
CAS No.:108293-72-7
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

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Technology Process of 1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

There total 1 articles about 1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 938-45-4
2-propionyl-p-cresol

: 106-95-6
allyl bromide

: 108293-72-7
1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

Guidance literature:: With potassium carbonate; In acetone; for 72h; Heating;
DOI:10.1021/jo00388a018

Reference yield:

: 108293-72-7
1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

: 108293-99-8
3,3'-(4-phenyl-2,6-pyridinediyl)bis(2-methoxy-5-methylbenzaldehyde)

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / 20 h / 190 °C

2: 96 percent / aq. KOH / tetrahydrofuran / 3 h / Heating

3: 16 percent / boron trifluoride etherate / 2 h / 70 °C

4: 80 percent / ammonium acetate / acetic acid / 3 h / Heating

5: 83 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; tetrahydrofuran / 18 h / Heating

6: 1.) ozone, 2.) I₂ / 1.) methanol, 3 h, 2.) methanol, glacial acetic acid, RT, 10 min

With ammonium acetate; potassium hydroxide; boron trifluoride diethyl etherate; potassium tert-butylate; iodine; ozone; In tetrahydrofuran; acetic acid; tert-butyl alcohol;
DOI:10.1021/jo00388a018

Reference yield:

: 108293-72-7
1-<5-methyl-2-(2-propenyloxy)phenyl>-1-propanone

: 108294-05-9
2,6-bis<3-(bromomethyl)-2-methoxy-5-methylphenyl>-4-phenylpyridine

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / 20 h / 190 °C

2: 96 percent / aq. KOH / tetrahydrofuran / 3 h / Heating

3: 16 percent / boron trifluoride etherate / 2 h / 70 °C

4: 80 percent / ammonium acetate / acetic acid / 3 h / Heating

5: 83 percent / potassium tert-butoxide / 2-methyl-propan-2-ol; tetrahydrofuran / 18 h / Heating

6: 1.) ozone, 2.) I₂ / 1.) methanol, 3 h, 2.) methanol, glacial acetic acid, RT, 10 min

7: 95 percent / sodium borohydride / ethanol / 1.) 20 min, 2.) RT, 30 min

8: 82 percent / phosphorus tribromide / benzene / 16 h / Ambient temperature

With ammonium acetate; potassium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; potassium tert-butylate; iodine; phosphorus tribromide; ozone; In tetrahydrofuran; ethanol; acetic acid; tert-butyl alcohol; benzene;
DOI:10.1021/jo00388a018