methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate

Base Information

Chemical Name:methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate
CAS No.:1034151-95-5
Molecular Formula:C₃₈H₃₁Cl₂NO₄
Molecular Weight:636.574
Hs Code.:

Synonyms:methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate

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Chemical Property of methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate

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Technology Process of methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate

There total 2 articles about methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1468-95-7
9-hydroxymethylanthracene

: C₁₄H₁₁Cl₂NO

: 22979-35-7
Methyl phenyldiazoacetate

: 1034151-95-5
methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate

Guidance literature:: With dirhodium tetraacetate; C₄₀H₂₅O₄P; In dichloromethane; at -20 ℃; for 3h; optical yield given as %ee; enantioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja801755z

Reference yield: 95.0%

: 1468-95-7
9-hydroxymethylanthracene

: 22979-35-7
Methyl phenyldiazoacetate

: 303771-70-2
C₁₄H₁₁Cl₂NO

: 1034151-95-5
methyl (2S,3S)-2-(9-anthrylmethoxy)-3-(4-methoxyphenylamino)-3-(2,3-dichlorophenyl)-2-phenylpropanoate

Guidance literature:: 9-hydroxymethylanthracene; C₁₄H₁₁Cl₂NO; With dirhodium tetraacetate; (R)‐3,3′‐bis(9‐phenanthryl)‐1,1′‐binaphthalene‐2,2′‐diyl hydrogen phosphate; In dichloromethane; at 23 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

Methyl phenyldiazoacetate; In dichloromethane; at -20 ℃; for 3h; enantioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.15227/orgsyn.088.0418