2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol

Base Information

• Chemical Name: 2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol
• CAS No.: 1053223-32-7
• Molecular Formula: C₁₇H₂₁NO₆
• Molecular Weight: 335.357

Synonyms:2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol

Chemical Property of 2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol

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Technology Process of 2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol

There total 1 articles about 2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-methyl-4,5-(3-O-acetyl-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline (257927-02-9) → 2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol (1053223-32-7)

Guidance literature:

With 10% Pd on charcoal; hydrogen; In tetrahydrofuran; methanol; at 20 ℃;

DOI:10.1021/jo801037z

Reference yield: 94.0%

2-acetamido-3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-glucitol (1053223-32-7) + p-toluenesulfonyl chloride (98-59-9) → 3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-2-p-tosylamino-D-glucitol (1223105-67-6)

Guidance literature:

With pyridine; for 30h; Reflux;

DOI:10.1021/jo100456z

upstream raw materials:

2-methyl-4,5-(3-O-acetyl-4,6-O-benzylidene-1,2-dideoxy-α-D-glucopyrano)[2,1-d]-2-oxazoline

Downstream raw materials:

3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-2-p-tosylamino-D-glucitol

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