Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester
CAS No.:109640-03-1
Molecular Formula:C₂₁H₃₁NO₄S
Molecular Weight:393.547
Hs Code.:

Synonyms:Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester

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Technology Process of Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester

There total 2 articles about Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 109639-93-2
cis-N,N-diisopropyl-4-(hydroxymethyl)cyclohex-2-enecarboxamide

: 98-59-9
p-toluenesulfonyl chloride

: 109640-03-1
Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester

Guidance literature:: With pyridine; at -10 ℃; for 7h;
DOI:10.1021/ja00252a016

Reference yield:

: 87115-25-1
(N,N-Diisopropylcarboxamido)cyclohex-3-ene

: 109640-03-1
Toluene-4-sulfonic acid (1S,4R)-4-diisopropylcarbamoyl-cyclohex-2-enylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 74 percent / pyridine / 7 h / -10 °C

With pyridine;
DOI:10.1021/ja00252a016