Technology Process of C19H26N2O2
There total 7 articles about C19H26N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; trichlorophosphate;
at 0 - 23 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 85 °C / Inert atmosphere
2.1: hydrogen / platinum(IV) oxide / ethanol; acetic acid
3.1: potassium hydroxide; water / ethanol / 3 h / 70 °C
3.2: pH 4
4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 23 °C / Inert atmosphere
5.1: ammonium hydroxide / dichloromethane; water / 0.25 h
6.1: pyridine; trichlorophosphate / 3 h / 0 - 23 °C / Inert atmosphere
With
pyridine; ammonium hydroxide; oxalyl dichloride; water; hydrogen; potassium carbonate; potassium hydroxide; trichlorophosphate;
platinum(IV) oxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N,N-dimethyl-formamide;
In
ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 85 °C / Inert atmosphere
2.1: hydrogen / platinum(IV) oxide / ethanol; acetic acid
3.1: potassium hydroxide; water / ethanol / 3 h / 70 °C
3.2: pH 4
4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 23 °C / Inert atmosphere
5.1: ammonium hydroxide / dichloromethane; water / 0.25 h
6.1: pyridine; trichlorophosphate / 3 h / 0 - 23 °C / Inert atmosphere
With
pyridine; ammonium hydroxide; oxalyl dichloride; water; hydrogen; potassium carbonate; potassium hydroxide; trichlorophosphate;
platinum(IV) oxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N,N-dimethyl-formamide;
In
ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;