Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)-

Base Information

Chemical Name:Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)-
CAS No.:147744-85-2
Molecular Formula:C₂₂H₄₁As₂B
Molecular Weight:466.222
Hs Code.:
DSSTox Substance ID:DTXSID301223943

Synonyms:Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)-;DTXSID301223943;147744-85-2

Suppliers and Price of Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:7
Exact Mass:466.17332
Heavy Atom Count:25
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B(C1=CC=CC=C1)([As](C(C)(C)C)C(C)(C)C)[As](C(C)(C)C)C(C)(C)C

Technology Process of Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)-

There total 1 articles about Arsine, (phenylborylene)bis[bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 148098-61-7
(C₆H₅BClAs(C(CH₃)3)2)2

: 19966-87-1
(di-tert-butylarsino)lithium

: 147744-85-2
C₆H₅B(As(C(CH₃)3)2)2

Guidance literature:: In diethyl ether; hexane; Schlenk technique or drybox under N2; a soln. of the boron-compd. in Et2O is treated via cannula with t-Bu2AsLi in hexane, soln. is stirred overnight; solvents are removed under reduced pressure, the residue is extd. with hexane, filtered and concd. and stored overnight in a -20°C freezer, crystn.;
DOI:10.1021/ja00061a021