(S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

Base Information

Chemical Name:(S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester
CAS No.:796869-93-7
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:(S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

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Chemical Property of (S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

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Technology Process of (S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

There total 1 articles about (S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4224-69-5
methyl 2-(bromomethyl)propenoate

: 65926-39-8
(R)-benzyl 2-(((benzyloxy)carbonyl)amino)-3-iodopropanoate

: 796869-93-7
(S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

Guidance literature:: (R)-benzyl 2-(((benzyloxy)carbonyl)amino)-3-iodopropanoate; With zinc; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

methyl 2-(bromomethyl)propenoate; In N,N-dimethyl-formamide; Further stages.;
DOI:10.1016/j.tetlet.2004.09.033

Reference yield: 64.0%

: 17510-52-0
sodium chloro(ethoxycarbonyl)chloroamide

: 796869-93-7
(S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

: (S)-5-Benzyloxycarbonylamino-2-(ethoxycarbonylamino-methyl)-2-hydroxy-hexanedioic acid 6-benzyl ester 1-methyl ester

Guidance literature:: With Hydroquinone 1,4-phthalazinediyl diether; potassium dioxotetrahydroxoosmate(VI); In acetonitrile; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2004.09.033

Reference yield: 53.0%

: 73210-14-7
N-chloro-N-sodio-tert-butylcarbamate

: 796869-93-7
(S)-2-Benzyloxycarbonylamino-5-methylene-hexanedioic acid 1-benzyl ester 6-methyl ester

: 5-benzyloxycarbonylamino-2-(tert-butoxycarbonylamino-methyl)-2-hydroxy-hexanedioic acid 6-benzyl ester 1-methyl ester

Guidance literature:: With Hydroquinone 1,4-phthalazinediyl diether; potassium dioxotetrahydroxoosmate(VI); In acetonitrile; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2004.09.033