5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate

Base Information

• Chemical Name: 5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate
• CAS No.: 121256-17-5
• Molecular Formula: C₇₀H₆₆ClN₆O₁₄PS₂
• Molecular Weight: 1345.88

Synonyms:5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate

Chemical Property of 5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate

Chemical Property:

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Technology Process of 5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate

There total 4 articles about 5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C70H66ClN6O14PS (121238-16-2) → 5'-O-dimethoxytrityl-N4-toluyldeoxycytidinyl-3'-O-(5'-O-N4-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate (121256-17-5)

Guidance literature:

With sulfur; In chloroform; toluene; Yield given;

DOI:10.1016/S0040-4039(00)95248-1

Reference yield:

5'-O-dimethoxytrityl-N4-toluyldeoxycitidine (95900-42-8) → 5'-O-dimethoxytrityl-N4-toluyldeoxycytidinyl-3'-O-(5'-O-N4-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate (121256-17-5)

Guidance literature:

Multi-step reaction with 4 steps

2: tetrazole

3: tetrazole / acetonitrile / 0.5 h

4: sulfur / CHCl₃; toluene; various solvent(s)

With 1H-tetrazole; sulfur; In chloroform; toluene; acetonitrile;

DOI:10.1016/S0040-4039(00)95248-1

Reference yield:

C50H64N5O7P (121238-14-0) → 5'-O-dimethoxytrityl-N4-toluyldeoxycytidinyl-3'-O-(5'-O-N4-toluyldeoxycytidine-3'-O-phenoxyacetyl)-S-(4-chlorobenzyl)phosphorodithioate (121256-17-5)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrazole

2: tetrazole / acetonitrile / 0.5 h

3: sulfur / CHCl₃; toluene; various solvent(s)

With 1H-tetrazole; sulfur; In chloroform; toluene; acetonitrile;

DOI:10.1016/S0040-4039(00)95248-1

upstream raw materials:

C₇₀H₆₆ClN₆O₁₄PS

5'-O-dimethoxytrityl-N₄-toluyldeoxycitidine

C₅₀H₆₄N₅O₇P

5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidinyl-3'-O-phenoxyacetyl)diisopropylphosphoramidite

Downstream raw materials:

5'-O-dimethoxytrityl-N4-toluyldeoxycytidine-3'-O-(5'-O-N4-toluyldeoxycytidine-3'-O-β-cyanoethyl-N,N-diisopropylaminophosphine)-S-(4-chlorobenzyl)phosphorodithioate

5'-O-dimethoxytrityl-N₄-toluyldeoxycytidinyl-3'-O-(5'-O-N₄-toluyldeoxycytidinyl)-S-(4-chlorobenzyl)phosphorodithioate

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