C₅₃H₄₆N₆O₇

Base Information

• Chemical Name: C₅₃H₄₆N₆O₇
• CAS No.: 1588471-68-4
• Molecular Formula: C₅₃H₄₆N₆O₇
• Molecular Weight: 878.984
• Mol file: 1588471-68-4.mol

Synonyms:C₅₃H₄₆N₆O₇

Chemical Property of C₅₃H₄₆N₆O₇

Chemical Property:

Purity/Quality:

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Technology Process of C₅₃H₄₆N₆O₇

There total 1 articles about C₅₃H₄₆N₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) → C53H46N6O7 (1588471-68-4)

Guidance literature:

Multi-step reaction with 5 steps

1: acetic acid / 5 h / 110 °C

2: trifluoroacetic acid; hydrogenchloride / 20 h / 74 °C / Inert atmosphere; Reflux

3: zinc(II) chloride; sodium cyanoborohydride / methanol / 12 h / 20 °C / Inert atmosphere

4: sulfuryl dichloride / dichloromethane / 20 °C / Inert atmosphere

5: triethylamine / dichloromethane / 48 h / 20 °C

With hydrogenchloride; sulfuryl dichloride; sodium cyanoborohydride; triethylamine; trifluoroacetic acid; zinc(II) chloride; In methanol; dichloromethane; acetic acid;

DOI:10.1021/ol5007339

Reference yield: 70.0%

C53H46N6O7 (1588471-68-4) → C37H42N6O3 (1588471-71-9)

Guidance literature:

C₅₃H₄₆N₆O₇; With hydrazine hydrate; In ethanol; for 2h; Reflux;

With sodium hydroxide; In water; at 20 ℃; for 0.75h;

DOI:10.1021/ol5007339

upstream raw materials:

phthalic anhydride

Downstream raw materials:

C₃₇H₄₂N₆O₃