2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

Base Information

Chemical Name:2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate
CAS No.:1258947-49-7
Molecular Formula:C₄₄H₃₂N₄O₄
Molecular Weight:680.762
Hs Code.:

Synonyms:2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

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Chemical Property of 2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

Chemical Property:

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Technology Process of 2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

There total 7 articles about 2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1258947-42-0
3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)phenol

: 4513-56-8,27136-26-1,62211-77-2
2-bromoethyl methacrylate

: 1258947-49-7
2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/cm201562p

Reference yield:

: 1711-05-3
m-anisoyl chloride

: 1258947-49-7
2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

1.2: 0.75 h

2.1: trichlorophosphate / 100 °C

3.1: copper; potassium carbonate / N,N-dimethyl-formamide / 150 °C

4.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

5.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With boron tribromide; copper; potassium carbonate; trichlorophosphate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/cm201562p

Reference yield:

: 14266-19-4
3,5‐diiodobenzoic acid methyl ester

: 1258947-49-7
2-(3-(5-(3,5-bis(carbazol-9-yl)phenyl)-1,3,4-oxadiazol-2-yl)-phenoxy)ethyl methacrylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrazine hydrate / ethanol / Reflux

2.1: tetrahydrofuran; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2.2: 0.75 h

3.1: trichlorophosphate / 100 °C

4.1: copper; potassium carbonate / N,N-dimethyl-formamide / 150 °C

5.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

6.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With boron tribromide; copper; potassium carbonate; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/cm201562p