2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole

Base Information

Chemical Name:2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole
CAS No.:1333344-02-7
Molecular Formula:C₃₇H₃₃NS₂
Molecular Weight:555.808
Hs Code.:

Synonyms:2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole

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Chemical Property of 2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole

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Technology Process of 2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole

There total 1 articles about 2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1333343-97-7
C₂₂H₂₃NS₂

: 183270-58-8
2-phenyl-2-(2-pehnylethynyl)-1,3-dithiolane

: 1333344-02-7
2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole

Guidance literature:: 2-phenyl-2-(2-pehnylethynyl)-1,3-dithiolane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

C₂₂H₂₃NS₂; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; for 1h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201100111

Reference yield: 52.0%

: 1333344-02-7
2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole

: 538-51-2
benzylidene phenylamine

: 1333344-03-8
3-butyl-1,2-diphenyl-5-[4-(1,3,5-triphenyl-1H-pyrrol-2-yl)phenyl]-1H-pyrrole

Guidance literature:: 2-{4-[2-(hex-1-yn-1-yl)-1,3-dithiolan-2-yl]phenyl}-1,3,5-triphenyl-1H-pyrrole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

benzylidene phenylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; for 1h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201100111