4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

Base Information

Chemical Name:4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene
CAS No.:124201-32-7
Molecular Formula:C₁₇H₁₈N₂O₈
Molecular Weight:378.339
Hs Code.:

Synonyms:4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

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Technology Process of 4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

There total 3 articles about 4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 124201-31-6
trans-4-(3,4-(Methylenedioxy)-6-nitrophenyl)-5-nitrocyclohexene

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 124201-32-7
4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; tert-butyl alcohol; at 20 ℃; for 48h;
DOI:10.1021/jo00291a029

Reference yield:

: 124201-30-5
trans-1-(3,4-(Methylenedioxy)-6-nitrophenyl)-2-nitroethene

: 124201-32-7
4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / hydroquinone / toluene / 168 h / 130 °C

2: 86 percent / Triton-B / tetrahydrofuran; 2-methyl-propan-2-ol / 48 h / 20 °C

With N-benzyl-trimethylammonium hydroxide; hydroquinone; In tetrahydrofuran; toluene; tert-butyl alcohol;
DOI:10.1021/jo00291a029

Reference yield:

: 712-97-0
6-nitro-1,3-benzodioxole-5-carbaldehyde

: 124201-32-7
4-(2-Carbomethoxyethyl)-5-(3,4-(methylenedioxy)-6-nitrophenyl)-4-nitrocyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / KF

2: 75 percent / hydroquinone / toluene / 168 h / 130 °C

3: 86 percent / Triton-B / tetrahydrofuran; 2-methyl-propan-2-ol / 48 h / 20 °C

With potassium fluoride; N-benzyl-trimethylammonium hydroxide; hydroquinone; In tetrahydrofuran; toluene; tert-butyl alcohol;
DOI:10.1021/jo00291a029