N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide
CAS No.:1258311-51-1
Molecular Formula:C₁₆H₂₁NO₃S
Molecular Weight:307.414
Hs Code.:

Synonyms:N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

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Technology Process of N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

There total 1 articles about N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.9%

: 75-07-0,9002-91-9
acetaldehyde

: 152453-97-9
N-(but-3-en-1-yl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

: 1258311-51-1
N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: N-(but-3-en-1-yl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

acetaldehyde; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja1088452

Reference yield: 91.0%

: 1258311-51-1
N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

: 1-{3-[(4-methylphenyl)sulfonyl]-3-azabicyclo[4.1.0]hept-1-yl}propan-2-one

Guidance literature:: N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide; With (Ind)RuCl(PPh₃)2; camphor-10-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere;

With indium(III) triflate; In tetrahydrofuran; at 66 ℃; for 17h; Inert atmosphere;
DOI:10.1021/ja1088452

Reference yield:

: 1258311-51-1
N-(but-3-en-1-yl)-N-(4-hydroxypent-2-yn-1-yl)-4-methylbenzenesulfonamide

: 1-[(1S,6R)-(3-tosyl-3-azabicyclo[4.1.0]heptan-1-yl)]propan-2-one

: 1-[(1R,6S)-(3-tosyl-3-azabicyclo[4.1.0]heptan-1-yl)]propan-2-one

Guidance literature:: With F₆P^(1-)*C₁₉H₂₅N₂O₂RuS⁽¹⁺⁾; In tetrahydrofuran; at 40 ℃; for 17h; Solvent; Reagent/catalyst; Overall yield = 69 %; Overall yield = 24 mg; enantioselective reaction; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ja510968h