(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

Base Information

Chemical Name:(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate
CAS No.:847980-97-6
Molecular Formula:C₁₀₇H₁₁₂Cl₃NO₂₃
Molecular Weight:1886.42
Hs Code.:

(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

Synonyms:(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

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Chemical Property of (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

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Technology Process of (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

There total 1 articles about (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 847980-96-5
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl-(1->2)-4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranose

: 545-06-2
trichloroacetonitrile

: 847980-97-6
(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1039/b414119a

Reference yield: 60.0%

: 847980-97-6
(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

: 220734-77-0
(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-D-myo-inositol

: C₁₆₇H₁₇₅N₃O₃₃

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1039/b414119a

Reference yield: 53.0%

: 847980-97-6
(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl) trichloroacetimidate

: 1234177-46-8
(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-allyl-D-myo-inositol

: C₁₆₃H₁₇₃N₃O₃₃

: (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->2)-(4,6-di-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-allyl-D-myo-inositol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 0 ℃; for 0.5h; optical yield given as %de; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2010.04.014