[Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)^(2-)]

Base Information

• Chemical Name: [Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)^(2-)]
• CAS No.: 748781-65-9
• Molecular Formula: C₂₃H₁₉NO₄S₄*Ni
• Molecular Weight: 560.362

Synonyms:[Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)^(2-)]

Chemical Property of [Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)^(2-)]

Chemical Property:

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Technology Process of [Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)^(2-)]

There total 1 articles about [Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)^(2-)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

nickel(II) acetate tetrahydrate (6018-89-9) + [2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine] hydrochloride → [Ni(2,6-bis[2-mercapto-3-(methoxycarbonyl)-phenylthio]dimethylpyridine)(2-)] (748781-65-9)

Guidance literature:

With LiOCH₃; In tetrahydrofuran; methanol; under N2, Schlenk setup at room temp., ligand (0.74 mmol) in MeOH+THF treated with methanolic soln. of LiOCH3 (2.22 mmol), soln. filtered, metalsalt (0.64 mmol) in MeOH added dropwise; ppt. filtered off, washed (MeOH), dried (vac.), elem. anal.;

DOI:10.1002/ejic.200300519

upstream raw materials:

nickel(II) acetate tetrahydrate

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