Technology Process of C16H23NO5S
There total 7 articles about C16H23NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / Reflux
2: sulfuric acid / Reflux
3: trichlorophosphate; N,N-dimethyl-aniline; tetraethylammonium chloride / acetonitrile / 80 °C
4: sodium hydride / dimethyl sulfoxide / 80 °C
5: 3-chloro-benzenecarboperoxoic acid / dichloromethane
6: lithium hydroxide / 1,4-dioxane
With
sulfuric acid; tetraethylammonium chloride; sodium hydride; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; lithium hydroxide; trichlorophosphate;
In
1,4-dioxane; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.093
- Guidance literature:
-
C17H25NO5S;
With
lithium hydroxide; water;
In
1,4-dioxane;
at 20 ℃;
With
hydrogenchloride; water;
pH=2;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid / Reflux
2: trichlorophosphate; N,N-dimethyl-aniline; tetraethylammonium chloride / acetonitrile / 80 °C
3: sodium hydride / dimethyl sulfoxide / 80 °C
4: 3-chloro-benzenecarboperoxoic acid / dichloromethane
5: lithium hydroxide / 1,4-dioxane
With
sulfuric acid; tetraethylammonium chloride; sodium hydride; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; lithium hydroxide; trichlorophosphate;
In
1,4-dioxane; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.bmcl.2013.01.093
