bis(p-tolylthio)nickel

Base Information

• Chemical Name: bis(p-tolylthio)nickel
• CAS No.: 115896-71-4
• Molecular Formula: 2C₇H₇S*Ni
• Molecular Weight: 305.087

Synonyms:bis(p-tolylthio)nickel

Chemical Property of bis(p-tolylthio)nickel

Chemical Property:

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Technology Process of bis(p-tolylthio)nickel

There total 2 articles about bis(p-tolylthio)nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(acetylacetonate)nickel(II) + para-thiocresol (106-45-6) → bis(p-tolylthio)nickel (115896-71-4)

Guidance literature:

With HCCC(CH₃)2OH; In neat (no solvent); byproducts: 2-(p-methylphenyl)thio-3-hydroxy-3-methyl-1-butene; (Ar); addn. of 10 mmol of HCCC(CH3)2OH to 2 mol% of Ni(acac)2; stirring at room temp. for 5-10 min; addn. of CH3C6H4SH to the stirred mixt. at 5°C (water/ice bath); stirring for 10 min; heating at 60°C for 60 min;

DOI:10.1021/om051105j

Reference yield:

para-thiocresol (106-45-6) → bis(p-tolylthio)nickel (115896-71-4)

Guidance literature:

With ammonia; nickel(II) nitrate; unter Luftausschluss;

Reference yield: 83.0%

2-phenyl-2H-1,2,3-triazole 1-oxide (77896-39-0) + bis(p-tolylthio)nickel (115896-71-4) + para-thiocresol (106-45-6) → 2-phenyl-4-(p-tolylthio)-2H-1,2,3-triazole

Guidance literature:

With nickel(II) sulphate; caesium carbonate; N,N`-dimethylethylenediamine; In dimethyl sulfoxide; at 60 ℃; for 12h; regioselective reaction;

DOI:10.1039/c4ob02586e

upstream raw materials:

para-thiocresol

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