tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

Base Information

Chemical Name:tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate
CAS No.:134258-31-4
Molecular Formula:C₂₅H₄₇NO₆Si
Molecular Weight:485.737
Hs Code.:

Synonyms:tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

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Chemical Property of tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

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Technology Process of tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

There total 5 articles about tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 134271-33-3
tert-butyl -2,4-dideoxy-β-L-threo-hex-4-enopyranosid>uronate

: 134258-31-4
tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

: 134258-30-3,134285-85-1
tert-butyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-D-xylo-hexopyranuronate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 192h;
DOI:10.1002/hlca.19910740214

Reference yield:

: 33401-01-3,55652-76-1
benzyl 2-acetamido-3,4-di-O-acetyl-2-deoxy-α-D-glucopyranoside

: 134258-31-4
tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

Guidance literature:: Multi-step reaction with 5 steps

2: 93 percent / 7-methyl-1,5,7-triazabicyclo<4.4.0>dec-5-ene, molecular sieves (4 angstroem) / toluene / 3 h / Heating

3: 98 percent / 2.5 M NaOMe / methanol / 20 h

4: 93 percent / 2,6-dimethylpyridine / dimethylformamide / 24 h / Ambient temperature

5: 5 percent / H₂ / 10percent Pd-C / methanol / 192 h

With 2,6-dimethylpyridine; 4 A molecular sieve; hydrogen; sodium methylate; 1-methyl-2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19910740214

Reference yield:

: 134258-29-0
tert-butyl (benzyl 2-acetamido-2,4-dideoxy-β-L-threo-hex-4-enopyranosid)uronate

: 134258-31-4
tert-butyl <(cyclohexyl)methyl 2-acetamido-3-O-<(tert-butyl)dimethylsilyl>-2,4-dideoxy-α-D-xylo-hexopyranosid>uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 2,6-dimethylpyridine / dimethylformamide / 24 h / Ambient temperature

2: 5 percent / H₂ / 10percent Pd-C / methanol / 192 h

With 2,6-dimethylpyridine; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19910740214